Structure determination and phase transition behaviour of dimethyl sulfate

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Structure determination and phase transition behaviour of dimethyl sulfate.

The crystal structures of phase I and phase II of dimethyl sulfate, (CH3O)2SO2, have been determined using complementary high-resolution neutron powder and single-crystal X-ray diffraction techniques. Below its melting point of 241 K dimethyl sulfate crystallizes in an orthorhombic structure (I) in the space group Fdd2. On cooling below approximately 175 K the crystal transforms to a monoclinic...

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ژورنال

عنوان ژورنال: Acta Crystallographica Section B Structural Science

سال: 2006

ISSN: 0108-7681

DOI: 10.1107/s0108768106001893